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Beilstein J. Org. Chem. 2012, 8, 2149–2155, doi:10.3762/bjoc.8.242
Graphical Abstract
Scheme 1: Synthesis of glycoamino acid derivative 3 and its dimer, from the known mannopyranoside 1.
Scheme 2: To obtain the glycocystine derivative 3-dimer from the protected cysteine mannopyranoside precursor ...
Figure 1: In the 1H/13C HMBC NMR spectrum of the S-Fm-protected glycoamino acid derivative 8, protecting-grou...
Scheme 3: Proposed mechanism for the formation of S-Fm-protected 8 from N-Fmoc-protected 7 according to Rich ...
Beilstein J. Org. Chem. 2012, 8, 753–762, doi:10.3762/bjoc.8.86
Figure 1: Carbohydrate arrays on polystyrene slides can be obtained by noncovalent immobilisation of tritylat...
Scheme 1: Synthesis of the tritylated compounds 3 [28], 5 and 7: (a) dichloromethane, 2.5 h, rt, 98%, (b) HBTU/DI...
Figure 2: Comparison of the polystyrene and glass surfaces with and without aluminium backing by matrix-free ...
Scheme 2: The Man–Trt compound 5 forms the disulfide 8 during UV ionisation in MALDI-TOF MS analysis.
Figure 3: Limit-of-detection analysis of 5 on aluminium-backed glass and polystyrene slides. Both systems sho...
Figure 4: Comparison of MALDI-TOF MS spectra on the aluminium-backed polystyrene and glass slides after washi...
Figure 5: Photo of the aluminium strip on the back of the polystyrene support.